H. Matsumoto et al., Electron microscope observations of athermal omega-phase crystal formationand growth behaviors in a beta-Ti alloy cooled to 77 K, J JPN METAL, 63(6), 1999, pp. 806-807
It is known that omega-phase crystals in beta-Ti alloys are formed by quenc
hing, aging and stressing. It has also been predicted that athermal omega-p
hase crystals are formed by cooling from the negative temperature dependenc
e of electrical resistivity in the alloys at low temperature. In order to c
larify the formation of athermal omega-phase crystals formed by cooling, in
-situ dark field image observations of an as-quenched Ti-15 mass%Mo alloy w
ere carried out from room temperature to 77 K. In a specimen cooled to 77 K
without electron irradiation, the formation of athermal omega-phase crysta
ls was clearly observed, but when irradiated with electron beam the crystal
s were annihilated.