Thin pyrite (FeS2) films prepared by thermal-sulfurating iron films at various temperatures

Authors
Citation
L. Meng et Ms. Liu, Thin pyrite (FeS2) films prepared by thermal-sulfurating iron films at various temperatures, MAT SCI E B, 60(3), 1999, pp. 168-172
Citations number
19
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science","Material Science & Engineering
Journal title
MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY
ISSN journal
09215107 → ACNP
Volume
60
Issue
3
Year of publication
1999
Pages
168 - 172
Database
ISI
SICI code
0921-5107(19990629)60:3<168:TP(FPB>2.0.ZU;2-F
Abstract
The structure and morphology of polycrystalline FeS2 thin films prepared by sulfurating iron films sputtered on glass substrates are reported. The eff ect of sulfidation temperature on the formation of the FeS2 thin films has been investigated under 80 kPa sulfur pressure and 20 h annealing time. The re is a nearly complete transformation from iron into polycrystalline FeS2 between 400-600 degrees C sulfidation. Moreover, the film of 400 degrees C sulfidation has approximate FeS2 stoichiometrical composition and uniform m icrostructure. With tile increase in sulfidation temperature, the grain siz e and amount of FeS2 crystallises increase. (C) 1999 Elsevier Science S.A. All rights reserved.