Y. Morioka et Y. Tomota, ENHANCEMENT OF SHAPE-MEMORY AND ITS ANISO TROPY BY TRAINING TREATMENTIN AN FE-32MN-6SI ALLOY, Tetsu to hagane, 83(6), 1997, pp. 389-394
The improvement of shape memory effect due to the austenite (gamma) re
versible arrow epsilon (epsilon) martensitic transformations and the d
evelopment of its anisotropy by training treatment were studied by usi
ng an Fe-32Mn-6Si alloy. The training treatment of five times repetiti
ons of 2% tensile deformation at 300K and heating up to 723K was given
to the solution-treated samples. By this treatment, lots of stacking
faults are introduced in the samples. The test specimens were cut from
the trained plates either parallel (0 degrees sample) or vertical (90
degrees one) with respect to the training direction. In the 0 degrees
samples the pre-existing stacking faults are found to be very effecti
ve not only to produce the stress-induced epsilon martensite but also
to increase the gamma strength against usual slip. A seemingly one thi
ck epsilon plate has been revealed to consist of nano-scale gamma/epsi
lon lamellar structure which is preferable to hold the back stress. Th
e shape recovery improved due to the reversible motion of Shockley is
partial dislocations assisted by this back stress. The recovery stress
for backward motion of Shockley partial dislocations during the epsil
on-->gamma reversion is found to increase markedly by the training tre
atment. On the other hand. in the 90 degrees samples, the pre-existing
stacking faults are of no use to enhance the stress-induced epsilon m
artensitic transformation and they rather hinder the transformation. I
ntersections of epsilon/epsilon plates and/or epsilon plates/stacking
faults were frequently observed. Since the gamma is almost equally str
engthened in the 0 degrees and 90 degrees samples by the training, the
slight increase in the shape recovery strains in the 90 degrees sampl
es compared with the non-treated samples is presumably resulted from t
he existence of higher back stress.