The small-angle X-ray scattering beamline at ELETTRA: A new powerful station for fast structural investigations on complex fluids with synchrotron radiation
H. Amenitsch et al., The small-angle X-ray scattering beamline at ELETTRA: A new powerful station for fast structural investigations on complex fluids with synchrotron radiation, NUOV CIM D, 20(12BIS), 1998, pp. 2181-2190
Citations number
14
Categorie Soggetti
Physics
Journal title
NUOVO CIMENTO DELLA SOCIETA ITALIANA DI FISICA D-CONDENSED MATTER ATOMIC MOLECULAR AND CHEMICAL PHYSICS FLUIDS PLASMAS BIOPHYSICS
The double-focusing high-flux wiggler beamline dedicated to Small Angle and
Wide Angle X-ray Scattering (SAXS/WAXS) at ELETTRA has recently gone into
operation. It has been designed specifically for time-resolved (resolution
similar to 1 ms) structure investigations on gels, liquid crystals, (bio)po
lymers, amorphous materials, muscles and proteins in solution. The beamline
is working at 3 fixed energies, namely 5.4, 8 and 16 keV, therefore the be
amline is equally applicable to very thin (e.g., single muscle fibres) and
optically thick (alloys or ceramics, having high Z) specimen. At the photon
energy of 8 keV the SAXS-resolution ranges from 1 to about 140 nm in d-spa
cing, and the flux at the sample is 2 x 10(12) photons/s corresponding to a
flux density of 5 x 10(11) ph/s (ELETTRA: 2 GeV and 250 mA). It is also po
ssible to perform simultaneously nide-angle diffraction measurements in the
d-spacing range of 0.12 to 0.94 nm (at 8 keV). Typical spot sizes are 5.4
x 1.8 mm(2) at the sample and 1.2 x 0.6 mm(2) in the focal spot. A multi-pu
rpose sample stage allows to install a large variety of user-designed instr
umentation, in order to perform temperature scans and jumps, pressure scans
and jumps, shear and flow jump relaxation experiments, grazing incidence S
WAXS, micro-spot scanning SWAXS, as well as studies applying mechanical str
esses or magnetic fields.