MIC-SSMS analyses of eight new geological standard glasses

Citation
B. Stoll et Kp. Jochum, MIC-SSMS analyses of eight new geological standard glasses, FRESEN J AN, 364(5), 1999, pp. 380-384
Citations number
14
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY
ISSN journal
09370633 → ACNP
Volume
364
Issue
5
Year of publication
1999
Pages
380 - 384
Database
ISI
SICI code
0937-0633(199907)364:5<380:MAOENG>2.0.ZU;2-7
Abstract
To obtain suitable geological reference materials for microanalytical purpo ses, a set of eight natural glasses was prepared by direct fusion of rock c hips. Multi-ion counting spark source mass spectrometry (MIC-SSMS) has been applied for trace element analysis of these reference materials. The overa ll analytical uncertainty of the MIC-SSMS results was determined by conside ring 14 possible sources of errors. It generally ranges between < 2-7% depe nding on the element and its concentration. Nearly all MIC SSMS data agree with the reference values within 0-10%, indicating that the estimate of the overall analytical uncertainty is reasonable.