The thru-x-y (Txy) family of calibration techniques has been applied to the
measurement of the microwave-modulation response of optical components usi
ng the most generalized form of available algorithms. An automated bilatera
l optical test set has been developed for the purpose. A wide variety of re
sults demonstrating the good performance of the techniques applied to optic
al components are presented. The measured results are compared to find the
most suitable calibration technique in terms of accuracy. This work represe
nts the first comprehensive comparison of all the Txy family of calibration
techniques in the optical domain.