Earlier work that reported relationships between compression properties and
elevated-temperature aging duration and weight losses also pointed out the
apparent influence of surface layer formation and growth on the retention
of compression properties during extended aging times. Since that time, fur
ther studies have focused on evaluating the growth of the surface layer. Th
e composition and features of this layer were found to change as the aging
temperature changed. Microcracks and small voids initiated and advanced inw
ard at all temperatures. Visible oxidation at the surface occurred only at
temperatures above 260 degrees C. Relationships between layer thickness, ag
ing time, and temperature were evaluated and empirically formulated. Then,
the compression properties were graphically related to the surface layer th
ickness with excellent correlation.