The dielectric relaxation frequency, f(x), which is associated with bulk po
larization processes in Ni-Zn and Mn-Zn polycrystsaline ferrites, was inves
tigated by using impedance spectroscopy. The behavior of f(x) showed a clea
r maximum as a function of the temperature. This maximum agrees with Curie
temperature, which was determined by an independent magnetic technique. The
se results show that impedance spectroscopy can be effectively used to stud
y the ferri-paramagnetic transition.