The semiconductor industry started to conquer the nm-scale in process techn
ology to create the next generation of microsized integrated circuits. With
the down-scaling of semiconductor structures, surfaces and interfaces need
precise control to achieve high yielding integrated circuits. For roughnes
s determination of high quality surfaces and thickness control of ultra-thi
n layers, X-ray scattering proves to be an innovative tool. We demonstrate
that specular and diffuse X-ray scattering from a silicon surface with a th
in thermal oxide allows the precise determination of real structure paramet
ers such as roughness, bulk density, oxide thickness, lateral correlation l
ength and fractal dimension. (C) 1999 Elsevier Science B.V. All rights rese
rved.