Fresh and dry Peganum harmala from Morocco were investigated for volatile c
omponents. Thirty-one volatile constituents were identified from aerial org
ans (leaves and stems) and roots. The dry parts were qualitatively richer i
n volatiles than the fresh ones. The leaves contained more volatile molecul
es than stems and roots. The main constituents were propylic acid and 2,3-d
ihydiobenzofurane identified in both fresh and dry materials, 3-octanone pr
esent in the aerial parts, and isovanillin detected only in dry P. harmala
organs.