Synthesis and structure of a bis(ethynyl)-substituted oxahexacyclic cage ether

Authors
Bott, SG Marchand, AP Kumar, KA
Citation
Sg. Bott et al., Synthesis and structure of a bis(ethynyl)-substituted oxahexacyclic cage ether, J CHEM CRYS, 29(3), 1999, pp. 347-349
Citations number
17
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
ISSN journal
10741542 → ACNP
Volume
29
Issue
3
Year of publication
1999
Pages
347 - 349
Database
ISI
SICI code
1074-1542(199903)29:3<347:SASOAB>2.0.ZU;2-5
Abstract
Intramolecular dehydration of a cage-diol results in the title compound. Th is crystallizes in the monoclinic space group P2(1)/c; a = 8.6403(8), b = 9 .5698(7), c = 14.062(1) Angstrom beta = 107.47(7)degrees; and Z = 4.