Small Angle X-Ray Scattering is one of the few techniques suitable for the
determination of the grain size distribution of nanostructured materials. A
theoretical development has allowed us to determine the spatial self-corre
lation function of such systems and thus the scattering profile associated
with the grain size distribution in the SAXS spectra without supposing any
specific shape in the precipitates and taking into account their impingemen
t. It has been tested in the primary crystallization of the amorphous Fe73.
5Cu1Nb3Si17.5B5 giving excellent agreement with the experimental data. (C)
1999 Acta Metallurgica Inc.