ESTIMATION OF MEAN PARTICLE-SIZE FROM SINGLE SECTIONS

Citation
Lm. Karlsson et Lm. Cruzorive, ESTIMATION OF MEAN PARTICLE-SIZE FROM SINGLE SECTIONS, Journal of Microscopy, 186, 1997, pp. 121-132
Citations number
34
Categorie Soggetti
Microscopy
Journal title
ISSN journal
00222720
Volume
186
Year of publication
1997
Part
2
Pages
121 - 132
Database
ISI
SICI code
0022-2720(1997)186:<121:EOMPFS>2.0.ZU;2-T
Abstract
The usual size descriptors for three-dimensional (3D) particles are vo lume (V), surface area (S) and, to a lesser extent, mean height (H), t he mean being over isotropic directions in space. With these parameter s we can construct 12 weighted means for the particle population, name ly {E-Y(X), X = H, S, V and Y = N, H, S, V}, where E-Y(X) represents t he population mean of the parameter X weighted by the parameter Y. The ordinary means are the number-weighted ones, namely {E-N(X), X = H, S , V}, whose estimation is only possible using a 3D probe (notably the disector) to sample the particles. In this paper we describe a general strategy to estimate E-Y(X) and consider in detail the estimation of E-S(V) and E-V(S); unbiased estimators have been proposed for both wei ghted means from single or independent sections, but to our knowledge the corresponding sampling and estimation procedures have not yet been illustrated with real data. We do this here for the tungsten particle s in a cemented carbide.