Features of quantitative X-ray diffraction analysis of weakly absorbing powder products with a defective structure

Citation
Av. Kurdyumov et al., Features of quantitative X-ray diffraction analysis of weakly absorbing powder products with a defective structure, POWD MET ME, 37(11-12), 1998, pp. 659-664
Citations number
8
Categorie Soggetti
Metallurgy
Journal title
POWDER METALLURGY AND METAL CERAMICS
ISSN journal
10681302 → ACNP
Volume
37
Issue
11-12
Year of publication
1998
Pages
659 - 664
Database
ISI
SICI code
1068-1302(199811/12)37:11-12<659:FOQXDA>2.0.ZU;2-Q
Abstract
The methods of quantitative phase analysis of low-absorbing powders by X-ra y diffraction have been developed. The approach used accounts for the depen dence of line intensify absorption factor on the Bragg angle and sample por osity and thickness. If has been shown that the use of traditional methods without reference to this dependence results in considerable errors in quan titative determination of phase content and in phase structure investigatio n. The application of proposed methods is illustrated by phase analysis of products of boron nitride shock compression.