Rapid and clean synthesis of 5-arylhydrazones of Meldrum's acid using polymer supported Meldrum's acid anion

Citation
Bp. Bandgar et al., Rapid and clean synthesis of 5-arylhydrazones of Meldrum's acid using polymer supported Meldrum's acid anion, I J CHEM B, 38(6), 1999, pp. 721-723
Citations number
19
Categorie Soggetti
Organic Chemistry/Polymer Science
Journal title
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY
ISSN journal
03764699 → ACNP
Volume
38
Issue
6
Year of publication
1999
Pages
721 - 723
Database
ISI
SICI code
0376-4699(199906)38:6<721:RACSO5>2.0.ZU;2-#
Abstract
Polymer supported Meldrum's acid anion is treated with various aryl diazoni um fluoroborates at 25 degrees C in acetonitrile to give corresponding 5-ar ylhydrazones of Meldrum's acid in good yield. Isolation of pure products by simple filtration and evaporation is an important feature of this method.