Simple nitric acid leaching and alkali fusion techniques for the determinat
ion of the total content of fallout Pu-239,Pu-240 in deep-sea sediment were
compared. Leaching neither with boiling cone. HNO3 nor with boiling cone.
HNO3+H2O2 was found to be sufficient. The sodium hydroxide fusion technique
yielded reproducible analytical results and is proposed as an optimum diss
olution method for quantitative determination of the total content of fallo
ut Pu-239,Pu-240 in deep-sea sediment.