K. Matsuki et al., Effect of microstructure refinement on high strain rate superplasticity ina PM 2024Al-Fe-Ni alloy, MATER T JIM, 40(8), 1999, pp. 737-743
Improvement of high strain rate superplasticity (HSRS) of a high strength P
M 2024Al-3Fe-5Ni alloy has been examined in relation to the microstructure
refining through a modification of heating condition to testing temperature
s. The alloy was fabricated by an air atomization technique, followed by ex
trusion at 623 K and warm rolling at 523 K. After the warm rolling, the all
oy exhibited ultra fine-grained structure stabilized with a fine dispersion
of intermetallic particles. The high strain rate superplastic properties f
or the present alloy were remarkably improved by the microstructural refine
ment, even at the optimum superplastic temperature of 773 K, which is close
to the solidus temperature of about 780 K for the alloy. The finer the siz
es of matrix grains and intermetallic particles, the higher values of total
elongation and strain rate sensitivity were obtained at a high strain rate
range of 10(-1)-10 s(-1) and at a wide temperature range of 713-773 K. The
stress concentration during sliding at the particle/matrix interface was c
onsidered to be diffusionally relaxed, because the particles were sufficien
tly small. A constitutive equation has been obtained through an analysis of
high strain rate superplasticity data on the alloy. The high strain rate s
uperplastic mechanism for the alloy is probably lattice diffusion controlle
d grain boundary sliding.