A. Urena-fernandez et al., Interfacial characterization using transmission electron microscopy examination of the diffusion bonding of SiC whisker-reinforced aluminum alloys, J MATER RES, 14(3), 1999, pp. 811-816
This paper describes the microstructural characterization, using transmissi
on electron microscopy (TEM), of the solid-state, diffusion-bonded interfac
es generated in a SiC whisker-reinforced, aluminum composite. Diffusion bon
ding was carried out using an aluminum-lithium alloy as the bonding interla
yer. Two kinds of bonded interface were studied: those generated between th
e composite matrix and the metallic interlayer (metallic-metallic) and othe
r ceramic-metallic interfaces formed between the interlayer and the SiC whi
skers. The first showed the formation of zones of recrystallization across
the original bond interface, and the second generally presented a high degr
ee of continuity without the formation of interface reaction layers between
the SiC whiskers and the interlayer, However, the formation of a degradati
on oxide layer was detected in some of the whisker/interlayer diffusion bon
ds. Its presence is due to the reaction between the alloying elements of th
e AI-Li interlayer and the SiO2 layer which surround some of the whiskers o
f the parent composite.