Diffraction of 100 to 200 keV X-rays from an Si1-xGex gradient crystal: comparison with results from dynamical theory

Citation
S. Keitel et al., Diffraction of 100 to 200 keV X-rays from an Si1-xGex gradient crystal: comparison with results from dynamical theory, ACT CRYST A, 55, 1999, pp. 855-863
Citations number
19
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ACTA CRYSTALLOGRAPHICA SECTION A
ISSN journal
01087673 → ACNP
Volume
55
Year of publication
1999
Part
5
Pages
855 - 863
Database
ISI
SICI code
0108-7673(19990901)55:<855:DO1T2K>2.0.ZU;2-7
Abstract
In a large Czochralski-grown Si1-xGex (0.02 less than or equal to x less th an or equal to 0.07) gradient crystal, diffraction patterns have been measu red in symmetrical Laue geometry using synchrotron radiation in the energy range 100-200keV. The experimental data are in very good agreement with the results from geometrical optics theory for distorted crystals, if the crea tion of new wavefields for strain gradients larger than a critical value is taken into account. In this sense, the crystal behaves like an ideal gradi ent crystal. If the normal absorption is disregarded, for reflection 111 an d 100 keV energy, the full width at half-maximum values and the peak reflec tivities of the diffraction patterns range from 14.6 " and 97%, respectivel y, to 70.9 " and 74%, respectively, for a variation in the Ge concentration from 3.5 to 5.3 at.%.