Citation
Qy. Lu et al., Benzene-thermal co-reduction reaction for nanocrystalline intermetallics Fe3Si and Ni3Al, SOL ST ION, 124(3-4), 1999, pp. 317-321
Citations number
20
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science
Journal title
SOLID STATE IONICS
ISSN journal
01672738
→ ACNP
Volume
124
Issue
3-4
Year of publication
1999
Pages
317 - 321
Database
ISI
SICI code
0167-2738(199909)124:3-4<317:BCRFNI>2.0.ZU;2-6
Abstract
A co-reduction reaction was proposed to synthesize nanocrystalline intermet
allics Fe3Si and Ni3Al under benzene-thermal conditions, The reactions were
carried out in an autoclave at 450 degrees C using FeCl3 and SiCl4 or NiCl
2 and AlCl3 as reactants, respectively, and metal Na as a reductant. The pr
epared samples were characterized by X-ray diffraction (XRD) and transmissi
on electron microscopy (TEM). The possible formation process and the effect
ive factors of nanocrystalline intermetallic Fe,Si were discussed. (C) 1999
Published by Elsevier Science B.V. All rights reserved.