Synthesis of 1-bromo-3-buten-2-one

Authors
Westerlund, A Carlson, R
Citation
A. Westerlund et R. Carlson, Synthesis of 1-bromo-3-buten-2-one, SYN COMMUN, 29(22), 1999, pp. 4035-4042
Citations number
7
Categorie Soggetti
Organic Chemistry/Polymer Science
Journal title
SYNTHETIC COMMUNICATIONS
ISSN journal
00397911 → ACNP
Volume
29
Issue
22
Year of publication
1999
Pages
4035 - 4042
Database
ISI
SICI code
0039-7911(1999)29:22<4035:SO1>2.0.ZU;2-B
Abstract
A synthetic method for 1-bromo-3-buten-2-one is given. The compound is prep ared through the following sequence: 2-butanone to 2-methyl-2-ethyl-1,3-dio xolane to 2-(1-bromoethyl)-2-bromomethyl-1,3-dioxolane to 2-bromomethyl-2-v inyl-1,3-dioxolane to the final product. Full experimental details includin g spectral data are given.