Am. Allan et al., Impact of grinder configurations on grinding rate, particle size, and trace element contamination of plant samples, COMM SOIL S, 30(15-16), 1999, pp. 2123-2135
Samples of varying abrasiveness, including rice hulls, rice straw, wheat gr
ain, orange leaves, and filter paper, were ground to pass a 0.5-mm screen i
n two cyclone mills (Tecator Cyclotec model 1093 and Newport Scientific mod
el 6200) with original and modified internal components. The ground samples
were then digested in nitric acid and analyzed for 12 elements by Inductiv
e Coupled Plasma (ICP) spectroscopy. Analysis of aluminum (Al), copper (Cu)
, iron (Fe), and zinc (Zn) showed that the amount of metal contamination fr
om each mill was related to the abrasiveness of the plant material and the
metal composition of the internal components of the mill. Least contaminati
on was achieved using the Newport Scientific 6260 mill fitted with a stainl
ess steel impeller and an abrasive steel strap with industrial diamonds set
in pure nickel. For abrasive samples such as rice hulls a stainless steel
impeller was about six times more durable than an aluminum impeller. The Ne
wport mill ground samples in less time and reduced plant dry matter to fine
r particles, but impeller wear caused more variation in the distribution of
particle size, than the Cyclotec mill.