The results of the first experiments with test samples, tool steel and
polycrystalline Sn carried out with the scanning photoemission micros
cope built on the ELETTRA storage ring in Trieste are presented and di
scussed. The scanning photoemission microscope uses a zone plate optic
al system for demagnification of the photon beam to submicron dimensio
ns. The present performance of the microscope in photoemission allows
elemental and chemical mapping and small-spot photoelectron spectrosco
py with lateral resolution better than 200 nm. The reported results sh
ow how photoemission microscopy can distinguish the spatial distributi
on of carbide phases with different Fe content at the surface of a too
l steel and the correlation between inhomogeneous oxidation of a polyc
rystalline Sn sample and its grain structure. (C) 1977 by John Wiley &
Sons, Ltd.