J. Ahmed et al., Study of dislocation structures near fatigue cracks using electron channelling contrast imaging technique (ECCI), J MICROSC O, 195, 1999, pp. 197-203
The fatigue of copper single crystals, orientated for single slip, has been
studied using electron channelling contrast imaging in a scanning electron
microscope. With the incident beam set at the Bragg condition, changes in
the backscattered electron intensity occur as the beam is scanned over disl
ocations that cause a local tilting of the diffraction planes. This techniq
ue allows the evolution of dislocation structures over large areas to be fo
llowed through different stages of the fatigue life. Furthermore, it enable
s direct imaging of dislocation configurations at crack tips. The technique
is compared with transmission electron microscopy and electron backscatter
diffraction in its application to fatigue studies.