An optical layout for performing photoemission microscopy using synchrotron
light from the storage ring Elettra is described. The microscope, property
of the Technical University of Clausthal, was installed on an existing mon
ochromator and the light is deflected and focused by two toroidal mirrors.
A light spot of similar to 30 mu m diameter and a photon energy range from
45 to 160 eV has been achieved. The light illuminates the sample in the mic
roscope at grazing incidence and chemical contrast is observed in photoemis
sion. Apart from the standard photoemission mode of operation with synchrot
ron radiation, surface NEXAFS spectra from microspot areas can be measured,
and an example is shown. Images can also be obtained with variable kinetic
energies (and therefore variable surface sensitivity) of the secondary ele
ctrons while working in NEXAFS mode. The obliquely incident soft X-rays cau
se shadows due to topography on the surface, which allows an estimate of th
e height of features. Three-dimensional islands give rise to Fresnel diffra
ction and many fringes may be visible. This effect and its consequences for
chemical imaging are discussed.