Determination of habit planes using trace widths in TEM

Citation
Mx. Zhang et al., Determination of habit planes using trace widths in TEM, MATER CHAR, 43(1), 1999, pp. 11-20
Citations number
27
Categorie Soggetti
Material Science & Engineering
Journal title
MATERIALS CHARACTERIZATION
ISSN journal
10445803 → ACNP
Volume
43
Issue
1
Year of publication
1999
Pages
11 - 20
Database
ISI
SICI code
1044-5803(199907)43:1<11:DOHPUT>2.0.ZU;2-7
Abstract
A simple and accurate method of determining the habit planes from the deter mination of beam and habit plane trace directions using Kikuchi line diffra ction patterns and the measurement of the thickness of the thin foil has be en developed. The thickness of the thin foil can be calculated from the mea surements of the widths of the habit plane trace at two different positions . The first orientation is with the foil normal to the electron beam (zero tilt) and the second one is where the foil has been tilted by a known amoun t about an axis parallel to the original trace at zero tilt. From the beam and the trace directions and thickness of the thin foil, the indices of the habit plane normal may be calculated. The technique has been tested using {111} annealing twin interfaces in stainless steel and shown to be capable of determining habit planes to within a degree or two. Extension of this me thod to the measurement of martensite habit planes is described. (C) Elsevi er Science Inc., 1999. All rights reserved.