A new chemical route to prepare nanocrystalline cobalt monoarsenide

Citation
C. Wang et al., A new chemical route to prepare nanocrystalline cobalt monoarsenide, MATER RES B, 34(7), 1999, pp. 1129-1133
Citations number
16
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science","Material Science & Engineering
Journal title
MATERIALS RESEARCH BULLETIN
ISSN journal
00255408 → ACNP
Volume
34
Issue
7
Year of publication
1999
Pages
1129 - 1133
Database
ISI
SICI code
0025-5408(199905)34:7<1129:ANCRTP>2.0.ZU;2-Y
Abstract
A low-temperature solvothermal reduction process to nanocrystalline CoAs is reported here. All the precursors are easily accessible. The formation and crystalline temperature of CoAs could be as low as 140 degrees C. Powder X -ray diffraction (XRD) shows a single phase of CoAs. The average particle s ize observed from transmission electron micrography (TEM) is about 18 nm. E lemental analysis and X-ray photoelectron spectroscopy (XPS) were utilized to determine the chemical composition of the product, (C) 1999 Elsevier Sci ence Ltd.