Four interpenetrating three-dimensional frameworks in the hydrogen-bonded structure of 5-hydroxyisophthalic acid-4,4 '-trimethylenedipyridine (1/1)

Authors
Wheatley, PS Lough, AJ Ferguson, G Glidewell, C
Citation
Ps. Wheatley et al., Four interpenetrating three-dimensional frameworks in the hydrogen-bonded structure of 5-hydroxyisophthalic acid-4,4 '-trimethylenedipyridine (1/1), ACT CRYST C, 55, 1999, pp. 1486-1489
Citations number
17
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
ISSN journal
01082701 → ACNP
Volume
55
Year of publication
1999
Part
9
Pages
1486 - 1489
Database
ISI
SICI code
0108-2701(19990915)55:<1486:FITFIT>2.0.ZU;2-H
Abstract
The 1:1 adduct of 5-hydroxyisophthalie acid and 4,4'-trimethylenedipyridine is a salt, [HNC5H4(CH2)(3)C5H4N](+).[HOC6H3(COOH)COO](-) (C13H15N2+. C8H5O 5-). The anions are linked into C(7) chains by means of O-H ... O hydrogen bonds [O ... O 2.734 (2) Angstrom and O-H ... O 176 degrees], and these cha ins are linked by the cations via O-H ... N and N-H ... O hydrogen bonds [O ... N 2.620(2) Angstrom, O-H ... N 175 degrees, N ... O 2.748(2) Angstrom and N-H ... O 176 degrees] into four identical but independent interpenetra ting three-dimensional frameworks.