P. Troche et al., Thermally driven shape instabilities of Nb/Cu multilayer structures: instability of Nb/Cu multilayers, THIN SOL FI, 353(1-2), 1999, pp. 33-39
The disintegration of Nb layers in Nb/Cu multilayers during heat treatments
was investigated by means of X-ray diffraction (XRD), transmission electro
n microscopy (TEM), and X-ray microscopy (XRM). Spherically shaped Nb parti
cles were observed after a heat treatment at 870 K for 3 h. The growth velo
city of the Nb particles depends strongly on the initial interface roughnes
s and the Nb layer thickness. The XRM investigations indicate a process of
self-assembly, leading to a non-statistical distribution of the particles.
Measurements of the superconducting properties of both annealed and non-ann
ealed samples, confirm the microstructural observations. (C) 1999 Published
by Elsevier Science Ltd. All rights reserved.