M. Ruzinsky et al., Addition-cyclization reactions of hexa-2,4-dienoyl isothiocyanate with amines and sodium hydrogen sulfide, CHEM PAP-CH, 53(4), 1999, pp. 260-264
1,3-Thiazin-4-one derivatives were synthesized by boron trifluoride-catalyz
ed intramolecular cyclization of N-substituted N'-(hexa-2,4-dienoyl)thioure
as and by the reaction of hexa-2,4-dienoyl isothiocyanate with sodium hydro
gen sulfide. The structure of the prepared compounds was confirmed by their
IR, H-1 and C-13 NMR spectra.