Kh. Chai et al., Effects of segregated sulfur on recrystallization texture and magnetic induction in thin-gauged 3% silicon steel, IEEE MAGNET, 35(5), 1999, pp. 3373-3375
During final annealing at 1200 degrees C under a high vacuum, changes in re
crystallization texture with final annealing time were observed in thin-gau
ged 3% Si-Fe alloys. In the alloy containing 30 ppm bulk sulfur, the recrys
tallization texture varied from the {111} <uvw> to the {001} <uvw> and fina
lly to the {110} <001> Goss texture, resulting in higher magnetic induction
than 1.90 T. The trough in magnetic induction, which corresponds to the re
latively high surface-segregated sulfur range, is due to the magnetically d
etrimental effect of those textures, i.e. the {111} <uvw> and the {001} <uv
w>. In the alloy containing 6 ppm bulk sulfur, the correlation between magn
etic induction and surface-segregated sulfur was the same as that in the ot
her alloy. These results clearly indicate that the surface energy induced r
ecrystallization in the thin-gauged 3% Si-Fe alloys is strongly affected by
the segregation and the evaporation of sulfur.