Quantitative analysis of crystallographic preferred orientation (texture) o
f very small volumes in fine-grained polycrystalline materials has been car
ried out with a monochromatic X-ray microbeam (less than or equal to 30 mu
m) at the microfocus beamline of the European Synchrotron Radiation Facilit
y (ESRF). The experimental procedure is described and illustrated with text
ures of rolled aluminium, aluminium and steel wires, polymer fibers and nat
ural bone material (apatite).