Sensory analysis and headspace gas chromatography-flame ionization detectio
n (GC-FID) analysis of liquid sugars (sucrose) designated for food-industri
al use were performed in order to elucidate which compounds are responsible
for perceived off-odors and off-flavors in liquid sugar. The liquid sugar
samples investigated had various kinds of off-odors and off-flavors that mi
ght influence the quality of any food product in which they might be used,
such as a jam or a soft drink. The sensory scores for the different attribu
tes and the levels of different volatile compounds as measured by GC were a
nalyzed for correlation using partial least-squares (PLS) analysis. A link
between sensory analysis and GC analysis was thereby established, and compo
unds critical for the odor and flavor were identified using MS (mass spectr
ometry). Approximately 10 compounds were found to be correlated with the de
fined sensory attributes. Among these compounds associated with the sensory
attributes were dimethyl disulfide, 2,6-dimethylpyrazine, 4-methoxyphenol,
and 2,5-dimethylfuran.