Structural study of the electrochemically synthesized binuclear complex bis{1-phenylglyoxal bis(3-piperidylthiosemicarbazone)zinc(II)}

Authors
Duran, ML Sousa, A Romero, J Castineiras, A Bermejo, E West, DX
Citation
Ml. Duran et al., Structural study of the electrochemically synthesized binuclear complex bis{1-phenylglyoxal bis(3-piperidylthiosemicarbazone)zinc(II)}, INORG CHIM, 294(1), 1999, pp. 79-82
Citations number
13
Categorie Soggetti
Inorganic & Nuclear Chemistry
Journal title
INORGANICA CHIMICA ACTA
ISSN journal
00201693 → ACNP
Volume
294
Issue
1
Year of publication
1999
Pages
79 - 82
Database
ISI
SICI code
0020-1693(19991102)294:1<79:SSOTES>2.0.ZU;2-9
Abstract
The binuclear complex bis{1-phenylglyoxal bis(3-piperidylthiosemicarbazone) zinc(II)}, [Zn(C20H26N6S2)](2) was synthesized using an electrochemical met hod, and has been structurally characterized. Crystal data for [Zn(C20H26N6 S2)](2): orthorhombic, space group Pbcn with a = 11.4785(6), b = 18.5478(7) , c = 20.1133(14) Angstrom, Z = 8, V = 4282.1(4) Angstrom(3), R-1 = 0.0433 on 4365 unique reflections. (C) 1999 Elsevier Science S.A. All rights reser ved.