N. Miyata et al., Mechanical behavior of bioactive inorganic filler-resin composite cements in a simulated body fluid: Effect of filler material, J CERAM S J, 107(10), 1999, pp. 935-943
Composite cements consisting of different pairs of inorganic filler-resin w
ere prepared by selecting CaO-SiO2-P2O5-CaF2 glass, glass-ceramic A-W and s
ilica glass powders as inorganic fillers, and combining each of them with b
isphenol-alpha-glycidyl methacrylate/triethylene glycol dimethacrylate (Bis
-GMA/TEGDMA)) resin. The mechanical behavior of each of the composite resin
cements was investigated by examining their fracture strength in a simulat
ed body fluid(SBF) as a function of both the soaking time and the stressing
rate. It was found that, among the composite cements studied, the CaO-SiO2
-P2O5-CaF2 glass-filled composite cement showed a rapid strength degradatio
n with increasing the soaking time in SBF and the highest sensitivity to ti
me-dependent fatigue in SBF. On the other hand, the strengths of the resin
cements filled with glass-ceramic A-W and silica glass particles did not va
ry with soaking time up to 336 d in SBF, Thus, glass-ceramic A-W and silica
glass can strengthen the resin cement without increasing the sensitivity t
o time-dependent fatigue in SBF. The glass-ceramic A-W can be used as a rel
iable inorganic filler for the composite cements with the Bis-GMA/TEGDMA re
sin, because of its bioactivity and good chemical stability.