R. Pantel et al., Circuit failure identification using focused ion beam and transmission electron microscopy characterisation techniques., MICROEL ENG, 49(1-2), 1999, pp. 181-189
In this paper we present the development and improvement of techniques used
in CNET Meylan during the last few years for localisation, cross sectionin
g and observation of circuit failure using focused ion beam, scanning and t
ransmission electron microscopy techniques. Failure analysis examples are g
iven to illustrate the methods used. Defect localisation is carried out usi
ng potential contrast and electrical testing. The imaging and ion milling c
apability of the focused ion beam technique is used for cross sectioning th
e failure area with an accurate control of the localisation. The physical o
bservation of defects on the cross section is carried out either in situ us
ing scanning ion microscopy or ex situ using electron beams. For higher res
olution the defective area is ion milled using the focused ion beam techniq
ue to produce a thin lamella containing the defect which can be then observ
ed with sub-nanometer spatial resolution using transmission electron micros
copy. Chemical analysis can also be carried out in the transmission electro
n microscope using electron energy loss spectroscopy and electron energy fi
ltering to complete the failure identification. The high resolution composi
tional maps give a clear identification of the materials in the defect area
and allows us to give some hypothesis about the origin of the circuit fail
ure.