Jg. Noudem et al., OPTIMIZATION OF TEXTURING PROCESS BY HOT-PRESSING OF BI-PB-SR-CA-CU-O(2223) CERAMICS, Physica. C, Superconductivity, 230(1-2), 1994, pp. 42-50
We have optimized a texturing process of Bi-Pb-Sr-Ca-Cu-O (2223) super
conducting ceramics by hot pressing. The Hoechst precursor powder has
been first pressurized at 1 GPa and then heated under uniaxial stress
up to 35 MPa, just below the melting temperature between 850 degrees C
and 857 degrees C. We have obtained large textured samples having cri
tical transport current densities J(c) as large as 2500 A/cm(2). In th
is work, we have optimized the stress value as well as the temperature
treatment on the basis of characterizations such as magnetization and
electrical-transport measurements.