We present an experimental piece of evidence of the excess small-angle-scat
tering in a nearly symmetric diblock copolymer. This phenomenon is observed
only in the two-phase coexistence region of the ordered and disordered pha
ses near the order-disorder transition temperature, using the ultra-small-a
ngle x-ray scattering method. This excess scattering is found to be caused
by the difference of the density between the ordered and disordered phases
in the coexistence region. [S1063-651X(99)50610-7].