Aluminium-aluminium nitride composites fabricated by melt infiltration under pressure

Citation
M. Chedru et al., Aluminium-aluminium nitride composites fabricated by melt infiltration under pressure, J MICROSC O, 196, 1999, pp. 103-112
Citations number
13
Categorie Soggetti
Multidisciplinary
Journal title
JOURNAL OF MICROSCOPY-OXFORD
ISSN journal
00222720 → ACNP
Volume
196
Year of publication
1999
Part
2
Pages
103 - 112
Database
ISI
SICI code
0022-2720(199911)196:<103:ANCFBM>2.0.ZU;2-H
Abstract
Aluminium-matrix composites containing similar to 55 vol.% AlN particles we re fabricated by melt infiltration of aluminium into an AlN preform under a pressure of up to 130 MPa. Two different AlN powders (H.C. Starck, Goslar, Germany, and ESK, Elektroschmelzwerk, Kempten, Germany) and four types of aluminium alloy (2024, 1070, 6060 and 5754) were used, The initial AlN powd ers were characterized by scanning electron microscopy. The composites were studied by light microscopy, scanning and transmission electron microscopi es and energy-dispersive X-ray spectroscopy. Particle-matrix interfaces wer e observed using high-resolution electron microscopy. As a result of the me lt infiltration process, the composites are very dense and the microstructu re shows a homogeneous distribution of the reinforcement. The interfaces ar e clean with very little porosity. Some Al2Cu precipitates were observed in the 2024 matrix.