Hot ductility curve of an austenitic stainless steel and importance of dynamic recrystallisation in determining ductility recovery at high temperatures
B. Mintz et al., Hot ductility curve of an austenitic stainless steel and importance of dynamic recrystallisation in determining ductility recovery at high temperatures, MATER SCI T, 15(10), 1999, pp. 1179-1185
The importance of dynamic recrystallisation in restoring ductility at the h
igh temperature end of the hot ductility though has been examined in an aus
tenitic stainless steel. Compression testing was used to establish the crit
ical strain for dynamic recrystallisation epsilon(c) for the temperature ra
nge 1000 to 850 degrees C using the same str ain rates of 3 x 10(-2), 3 x 1
0(-3), and 3 x 10(-4) s(-1) as had been used in previous work to establish
the hot tensile ductility curves. Specimens were heated first to 1175 ol 10
00 degrees C to give a coarse (240 mu m) and finer (80 mu m) grained steel
respectively. The flow stress data from the compression tests on the coarse
r grained material were used to obtain the str ain to the peak stress epsil
on(p) which could then be used to calculate the curve of epsilon(p) versus
temperature for use in establishing the temperature at which dynamic recrys
tallisation would first occur in a tensile test. For the coal se grained st
eel, the hot tensile tests had given ductility troughs for each strain rate
with minimum ductility occurring at 850 degrees C, the trough deepening an
d widening with decreasing strain rate. The trough was found to be associat
ed with the presence of coarse carbides situated at the boundaries. Below 8
50 degrees C, ductility recovered because grain boundary sliding was reduce
d. Above 850 degrees C, ductility improved since fewer carbides were precip
itated at the boundaries, facilitating dynamic recrystallisation. Recovery
in ductility at the high temperature end of the trough in the coarse graine
d condition was shown to occur at a temperature close to that at which the
base of the trough in the ductility curve intersected the curve of epsilon(
c) versus temperature, i.e. when dynamic recrystallisation was possible but
only for a strain rate of 3 x 10(-3) s(-1). At higher strain rates the red
uction in the rate of grain boundary sliding was sufficient to improve duct
ility without the necessity for dynamic recrystallisation, At lower strain
rates cracks were able to develop to such a degree that dynamic recrystalli
sation was not effective in improving ductility. Refining the grain size el
iminated the trough for all the strain rates examined. In this case the cal
culated curve of epsilon(p) or epsilon(c) versus temperature intersected th
e hot ductility curves at temperatures below the range examined, indicating
that dynamic recrystallisation always occur red. It was concluded that dyn
amic recrystallisation can have a major influence in restoring ductility at
the high temperature end of the trough. However, it must often be well adv
anced to be effective and ductility can recover without the necessity for d
ynamic recrystallisation, by increasing the strain rate, thus reducing the
amount of grain boundary sliding.