E. Balikci et al., Microstructure and texture effect on the thermal expansion of a variously aged polycrystalline superalloy IN738LC, MET MAT T A, 30(11), 1999, pp. 2803-2808
Thermal-expansion measurements of a suitably heat-treated and aged polycrys
talline superalloy, IN738LC, with various gamma' (Ni-3(Al, Ti, Nb)) precipi
tate microstructures and annealing textures, were carried out using procedu
res given in ASTM E228. The preferred orientation (PO) and elasticity modul
us of the alloy under the different microstructural conditions are correlat
ed to the thermal expansivity obtained. Thermal expansion was found to decr
ease with decreasing gamma' precipitate size. The microstructures with coar
se and medium-sized precipitates, with the [100]-PO (soft directions in the
fee Ni-based alloys) and low elasticity modulus values, yield the highest
thermal expansion. The microstructure with fine-sized precipitates has a lo
wer expansion coefficient at all temperatures, while the duplex-size (fine
+ medium) precipitate microstructure and the single-phase solution-treated,
supersaturated solid solution (SSS) condition show the lowest expansion co
efficients. The low expansivity is attributed to the prevalence of the [111
] and/or [131] POs in these specimens for the matrix phase and the expansio
n being along these relatively harder directions. Internal constraints to e
xpansion, which determine d alpha/dT, are postulated to result from disloca
tion substructures present in the microstructural constituents and at the p
recipitate-matrix interface.