5,5-DIMETHYL-4(R)-PHENYL-1,3,2-DIOXAPHOSPHORINANE, A NEW REAGENT FOR THE ENANTIOMERIC EXCESS DETERMINATION OF UNPROTECTED AMINO-ACIDS USINGP-31 NMR

Authors
HULST R ZIJLSTRA RWJ DEVRIES NK FERINGA BL
Citation
R. Hulst et al., 5,5-DIMETHYL-4(R)-PHENYL-1,3,2-DIOXAPHOSPHORINANE, A NEW REAGENT FOR THE ENANTIOMERIC EXCESS DETERMINATION OF UNPROTECTED AMINO-ACIDS USINGP-31 NMR, Tetrahedron : asymmetry, 5(9), 1994, pp. 1701-1710
Citations number
33
Categorie Soggetti
Chemistry Inorganic & Nuclear","Chemistry Inorganic & Nuclear","Chemistry Physical
Journal title
Tetrahedron : asymmetry → ACNP
ISSN journal
09574166
Volume
5
Issue
9
Year of publication
1994
Pages
1701 - 1710
Database
ISI
SICI code
0957-4166(1994)5:9<1701:5ANRFT>2.0.ZU;2-Z
Abstract
Diastereomeric amide derivatives of title phosphorinane 2 and unprotec ted amino acids are easily prepared in aqueous solutions, showing well separated signals in the P-31 NMR spectra allowing accurate e.e. dete rmination.