Crystal structure of triethylentetraammonium bis monohydrogenmonophosphatedihydrate, [NH3(CH2)(2)NH2(CH2)(2)NH2(CH2)(2)NH3](HPO4)(2)center dot 2H(2)O

Authors
Elaoud, Z Kamoun, S Mhiri, T Jaud, J
Citation
Z. Elaoud et al., Crystal structure of triethylentetraammonium bis monohydrogenmonophosphatedihydrate, [NH3(CH2)(2)NH2(CH2)(2)NH2(CH2)(2)NH3](HPO4)(2)center dot 2H(2)O, J CHEM CRYS, 29(5), 1999, pp. 541-545
Citations number
9
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
ISSN journal
10741542 → ACNP
Volume
29
Issue
5
Year of publication
1999
Pages
541 - 545
Database
ISI
SICI code
1074-1542(199905)29:5<541:CSOTBM>2.0.ZU;2-T
Abstract
The salt triethylentetraammonium bis monohydrogenmonophosphate dihydrate is monoclinic with the following unit cell dimensions: a = 8.462(1), b = 10.5 00(1), c = 9.520 Angstrom, beta = 99.297(1)degrees space group P2(1)/n with Z = 2. The structure was solved by the Patterson method and refined to fin al R value of 0.043 for 1590 independent reflections. The structure consist s of infinite parallel two-dimensional [(1) over bar 01] planes built of mu tually connected ions and water molecules by strong O-H ... O and N-H ... O hydrogen bonding.