Organic reactions in aqueous solution - part-X: Effect of sonication on the reaction of hexamethylenetetramine with dibenzoylmethane in the formationof alpha,alpha,gamma,gamma-tetrabenzoylpropane

Citation
Ss. Ali et al., Organic reactions in aqueous solution - part-X: Effect of sonication on the reaction of hexamethylenetetramine with dibenzoylmethane in the formationof alpha,alpha,gamma,gamma-tetrabenzoylpropane, J CHEM S P, 21(1), 1999, pp. 78-82
Citations number
19
Categorie Soggetti
Chemistry
Journal title
JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN
ISSN journal
02535106 → ACNP
Volume
21
Issue
1
Year of publication
1999
Pages
78 - 82
Database
ISI
SICI code
0253-5106(199903)21:1<78:ORIAS->2.0.ZU;2-A
Abstract
An intensive investigation of the reaction of hexamethylenetetramine with d ibenzoylmethane under varying conditions in methanol, ethanol and their mix tures with water, and also in water alone has been carried out The effect o f sonication an these reactions has also been studied The study has led to the development of a simple method for the synthesis of alpha,alpha,gamma,g amma-tetrabenzoylpropane in the theoretical yield, hitherto, not reported i n the literature. Methylene-bis-dibenzoylmethane thus obtained turned out t o be tautomeric in nature. It has not been reported in the literature so fa r. Its tautomeric nature has been established and is being reported for the first time.