In this study samples of AISI 4140 steel were pretreated by plasma nitridin
g: and coated with two different physical vapour deposited coatings (TIN an
d TiAlN). A hardened AISI 4140 sample and a coated sample were also include
d in the investigation. To examine the influence of the nitrided zone on th
e performance of the coating-substrate composite, two different nitriding c
onditions - a conventional 25% N-2 and an N-2-poor gas mixture - were used.
The specimens were investigated with respect to their microhardness, surfa
ce roughness, scratch adhesion and dry sliding wear resistance. Wear tests
in which the duplex-treated pins were mated to hardened ball bearing steel
discs were performed in a pin-on-disc machine under dry sliding conditions.
Metallography, scanning electron microscopy and profilometry were used to a
nalyse the worn surfaces in order to determine the dominant friction and we
ar characteristics of the samples investigated. The results show improved w
ear properties of the plasma-nitrided hard-coated specimens compared with u
ncoated and pre-hardened ones. Although previous investigations showed a ne
gative effect of the compound layer, it was found that a precisely controll
ed plasma nitriding process can lead to a dense, uniform and highly adheren
t compound layer with a positive effect on the wear properties of pre-nitri
ded and hard-coated AISI 4140 steel. (C) 1999 Elsevier Science S.A. All rig
hts reserved.