Ma. Mangan et al., Correlation between the crystallography and morphology of proeutectoid Widmanstatten cementite precipitates, ACT MATER, 47(17), 1999, pp. 4263-4274
Electron backscatter diffraction was used in conjunction with deep etching
to examine the relationship between the crystallography and three-dimension
al morphology of cementite precipitates in an Fe-1.34 wt% C-13.1 wt% Mn ste
el. Orientation relationships (ORs) between more than 200 proeutectoid Widm
anstatten cementite precipitates and the surrounding austenite were determi
ned to be on or very near either the well-known Pitsch OR or the Farooque-E
dmonds OR. Scanning electron microscopy of the same specimens after deep et
ching was used to determine the three-dimensional morphology of each of the
precipitates for which an OR was determined. These precipitates could be i
dentified as either monolithic plates or conglomerates of laths. Results sh
ow that monolithic plates consistently exhibit the Pitsch OR and conglomera
tes of laths have the Farooque-Edmonds OR, indicating that the precipitate
morphologies are dictated by their orientation relationships. Published by
Elsevier Science Ltd on behalf of Acta Metallurgica Inc.