Synthesis of Ln-Ba-Cu-O cuprates from mechanochemically activated mixtures

Authors
Panova, TI Malysheva, SI Savchenko, EP Glushkova, VB
Citation
Ti. Panova et al., Synthesis of Ln-Ba-Cu-O cuprates from mechanochemically activated mixtures, INORG MATER, 35(12), 1999, pp. 1274-1277
Citations number
6
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science
Journal title
INORGANIC MATERIALS
ISSN journal
00201685 → ACNP
Volume
35
Issue
12
Year of publication
1999
Pages
1274 - 1277
Database
ISI
SICI code
0020-1685(199912)35:12<1274:SOLCFM>2.0.ZU;2-X
Abstract
LnBa(2)Cu(3)O(7-x) and LnBa(2)Cu(4)O(8) high-T-c materials were synthesized from fine powders obtained by mechanochemical activation of the starting m ixtures. The heat-treatment conditions were shown to have a crucial effect on the structural perfection and chemical composition of the resultant high -T-c ceramics. According to thermogravimetric measurements, these materials are stable up to 830 degrees C.