Scanning system for high-energy electron diffractometry

Citation
As. Avilov et al., Scanning system for high-energy electron diffractometry, J APPL CRYS, 32, 1999, pp. 1033-1038
Citations number
20
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
JOURNAL OF APPLIED CRYSTALLOGRAPHY
ISSN journal
00218898 → ACNP
Volume
32
Year of publication
1999
Part
6
Pages
1033 - 1038
Database
ISI
SICI code
0021-8898(199912)32:<1033:SSFHED>2.0.ZU;2-X
Abstract
A new electron diffractometer with a diffraction-pattern scanning system in front of a fixed counter has been developed. Significant improvement was a chieved in the measured diffraction intensities by using fast electronics a nd additional control of the stability of the electron beam. The measuremen t of and accounting for the gear-frequency characteristic of the registrati on system was performed, and the signal accumulation mode for intensity mea surements together with advanced statistical data processing were employed. Good agreement between the experimental and Hartree-Fock structure factors for LiF, NaF and MgO was achieved (to avoid strong extinction effects, rat her thin polycrystalline films were used as samples).