CYCLIC ORGANOLEAD COMPOUNDS .4. SYNTHESIS AND MULTINUCLEAR NMR PROPERTIES OF 6-MEMBERED HETEROCYCLIC ORGANOLEAD COMPOUNDS

Authors
VANBEELEN DC VANRIJN J HERINGA KD WOLTERS J DEVOS D
Citation
Dc. Vanbeelen et al., CYCLIC ORGANOLEAD COMPOUNDS .4. SYNTHESIS AND MULTINUCLEAR NMR PROPERTIES OF 6-MEMBERED HETEROCYCLIC ORGANOLEAD COMPOUNDS, Silicon, germanium, tin and lead compounds, 20(1), 1997, pp. 37-45
Citations number
39
Categorie Soggetti
Chemistry Inorganic & Nuclear","Chemistry Inorganic & Nuclear
Journal title
Silicon, germanium, tin and lead compounds → ACNP
ISSN journal
07921241
Volume
20
Issue
1
Year of publication
1997
Pages
37 - 45
Database
ISI
SICI code
0792-1241(1997)20:1<37:COC.SA>2.0.ZU;2-7
Abstract
Several six-membered heterocyclic organolead compounds were synthesize d from the appropriate di-Grignard resp. organodilithio compounds and a (diorgano)lead dihalide. The compounds were investigated by multinuc lear NMR spectroscopy. Variable temperature H-1 NMR measurements revea led a conformational equilibrium. In the C-13 and Pb-207 NMR spectra s pecific effects caused by the presence of a lead atom in the ring syst em could be observed.