The polarographic and voltammetric behaviour of hexa[4-(phenylazo)phenoxy]c
yclotriphasphazene in tetrahydrofuran-water 50% (v/v) was studied at room t
emperature using various electrochemical techniques. In this study, the red
uction of the azo group to the amino group of the organophosphazenes compou
nd was observed as the electrode reaction. An electrode reaction mechanism
was suggested for the compound.